A method to improve the adhesion between zirconia and a resinous cement.
DOI:
https://doi.org/10.31984/oactiva.v7i2.736Keywords:
Fuerza de Adhesión, Tratamiento térmico, Zirconia, Adhesión en Odontología, Tratamiento de Superficie, Cemento Resinoso.Abstract
Heat can be a source of improve of bond strength (FU) of bonding agents between zirconia and a resin cement. Objective: To measure the FU of the bonding agents used to cement zirconia, when they have been heated at 75 and 1000 C. Materials and Methods: three commercially available coupling agents, Single Bond Universal (3M), Monobond-N (Ivoclar Vivadent) and Clearfil Ceramic Primer (Kuraray America Inc). They were heated at 750C and 1000C for 5 min, and a control group at room temperature of 240C was used. For bonding zirconia ceramic (Y-TZP) with a 10 MDP based resin cement. Microshear bond strength (µSBS) was determined for all materials. Statistical analysis was performed with a 3-way ANOVA with a Greenhouse-Geisser. A Tukey post-hoc test was performed. Through the microscope all the detached surfaces were analyzed to classify them as adhesive, cohesive and mixed and they were represented in percentages. Results: All chemical agents had a better performance of their immediate bond strength when subjected to heat treatment. Although their resistance decreased after aging, the final value was still high compared to the control group. Conclusion: Heating of the coupling agents proved to be effective in increasing their strength values, when used to bond a Y-TZP to a resinous cement in both cases, immediately and after aging.
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